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Prices and Yields of Long-Term U.S. Government Securities: 1920 1946 49. Short-Term American Interest Rates: 1900 1945 50. Corporate and Municipal Long-Term Bond Yields: 1946 1989 51. Prices and Yields of Long-Term U.S. Government Securities: 1946 1989 52. Short-Term American Interest Rates: 1946 1989 53A. Yields by Maturity Basic Yields of Prime Corporate Bonds: 1900 1975 53B. Yields by Maturity U.S. Government Bonds: 1950 1989 54. Yield Differentials in Basis Points According to Maturity: 1900 1989 55. Examples of Terms, Yields, and Yield Spreads of New Issues of High-Grade Corporate Bonds: 1900 1989 56. Yield Differentials Between Long-Term Government, Corporate, and Municipal Bonds: 1900 1989 57. U.S. Conventional Real Estate Mortgage Rates: 1900 1989 58. U.S. Consumer Credit Commercial Bank Rates: 1972 1989 59. Prices and Yields of Long-Term British Government Securities: Twentieth Century 60. Prices and Real Yields of Representative British Government Index-Linked Bonds, 1981 1989 61. Short-Term British Interest Rates: Twentieth Century 62. Prices and Yields of Long-Term French Government Securities: Twentieth Century 63. Short-Term French Interest Rates: Twentieth Century 64. Prices and Yields of Long-Term Dutch Government Securities: Twentieth Century 65. Short-Term Dutch Interest Rates: Twentieth Century 66. Prices and Yields of Long-Term Belgian Government Securities: Twentieth Century 67. Short-Term Belgian Interest Rates: Twentieth Century 68. Prices and Yields of Long-Term German Government Securities: Twentieth Century 69. Short-Term German Interest Rates: Twentieth Century 70. Italian Interest Rates: Annual Averages, Late Nineteenth and Twentieth Centuries 71. Swiss Interest Rates: Twentieth Century 72. Interest Rates in Sweden: Twentieth Century 73. Austrian, Norwegian, Danish, and Irish Interest Rates: Annual Averages, 1930 1989

The carbonyl double bond has not generally been susceptible to polymerization by radical initiators. There are two reasons for this behavior: (1) the carbonyl group is highly polarized and not prone to attack by a radical; and (2) most radicals are produced at temperatures above the ceiling temperatures of carbonyl monomers. There are, however, a few isolated cases of carbonyl polymerizations by radical initiators. Tri uoroacetaldehyde has been polymerized using benzoyl peroxide at 22 C. The polymerization is slow, with 18 h required to obtain 90% conversion [Bus eld and Whalley, 1965]. However uorothiocarbonyl monomers such as thiocarbonyl uoride have been polymerized at high rates by using a trialkylboron oxygen redox system at 78 C [Sharkey, 1975]. Thioacetone is also polymerized by this redox system.

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Radical polymerizations are observed with these monomers because the electronwithdrawing substituents on the carbonyl and thiocarbonyl group decrease its polarity (and polarizability). The greater susceptibility of the thiocarbonyl double bond to radical polymerization is due to the lower electronegativity of sulfur compared to oxygen. The thiocarbonyl group is less polar than the carbonyl group and more prone to attack by a radical. The successful radical polymerization of thiocarbonyl monomers is also due in large part to the low temperature initiation process employed. 5-6d End Capping

Spade bits are not for the usual thin plastics of circuit-bent toys. Reserve them for materials thicker than 3 16", such as custom Lucite enclosures and control panels.

Polyacetals are generally unstable at ambient or moderate temperatures because of facile depolymerization due to their low ceiling temperatures. This limits the commerical utility of most polyacetals. Polyformaldehyde (IUPAC: polyoxymethylene) is an exception to this generalization since its ceiling temperatures is higher than those of other polyacetals. Depolymerization occurs on heating when reactive carbanion or carbocation centers are formed by thermal bond scission at the hydroxyl end groups of polyoxymethylene (POM). The commercial utility of POM is increased when the temperature at which depolymerization occurs is increased, and this is accomplished by converting the less stable hydroxyl end groups into more stable ester groups by reaction with an anhydride:

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5-131

This reaction is referred to as end capping or end blocking The result is that reactive carbanion or carbocation centers do not form and depolymerization does not occur at the ceiling temperature of the polymer The polymer chains are end blocked from depolymerization The effective ceiling temperature is increased considerably above the ceiling temperature Acetic anhydride is the usual capping reagent The anionic polymerization formaldehyde to POM followed by end capping is carried out commerically POM (trade name: Delrin) is highly crystalline (60 77%) because of the ease of packing of the simple, polar polymer chains (Tm 175 C) The commercial products have number-average molecular weights of 20,000 70,000 (PDI $2) POM has a good combination of properties high strength; toughness; resistance to creep, fatigue, and abrasion; low coef cient of friction; and low moisture absorption and is used as an engineering plastic.

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